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MELTING AND DISSOLVING FLY ASH BY NaOH FOR THE REMOVAL OF IRON, CALCIUM AND OTHER IMPURITIES
Pages : [17] - [33]
Received : October 29, 2019; Revised January 13, 2020
Communicated by : Professor Ana Rosa Silva
Abstract
Mixture of fly ash and sodium hydroxide was calcined, which converted mullite the high-temperature stability phase containing silicon and aluminum oxides, and quartz into activated silica alumina phase, and they were dissolved by concentrated solution into soluble and The insoluble impurities including and were filtered out. Experimental results show that the optimum experimental conditions for the dissolution: temperature is 60°C, solution is used, liquid-solid mass ratio is 11:1, stirring time is 3h, and about 78.9% of silicon and 78.1% of aluminum are dissolved. The obtained pure silicon aluminum solution provides the raw material for preparing high-purity molecular sieves, and content of the prepared P type molecular sieve is only 0.25% and the content is only 0.066%.
Keywords
melting and dissolving of coal fly ash, removal of Fe, P molecular sieve.